By Stanley M. Roberts, Ivan V. Kozhevnikov, Eric Derouane(eds.)
The chemist has an enormous diversity of high-tech catalysts to exploit while operating in fine chemical synthesis however the catalysts are regularly challenging to exploit and require either time, ability and adventure to deal with appropriately. The Catalysts for tremendous Chemical Synthesis series contains established and proven methods which provide a special variety assets for chemists who paintings in natural chemistry.
"... of serious worth to artificial natural chemists..." (The Chemists, summer time 2003)
quantity three within the sequence makes a speciality of catalysts for carbon-carbon bond formation and provides sensible and detailed protocols on tips on how to use refined catalysts through the "inventors" and "developers" who created them. The combination of protocols and evaluate commentaries is helping the reader to simply and quickly understand and use the hot high-tech catalysts.Content:
Chapter 1 concerns of commercial wonderful Chemical Synthesis (pages 1–12): Mark W. Hooper
Chapter 2 Alkylation and Allylation adjoining to a Carbonyl staff (pages 13–33): Fumitoshi Kakiuchi, Satoshi Ueno, Naoto Chatani, Michael North, Jose A. Fuentes, Barry Lygo and Benjamin I. Andrews
Chapter three uneven Alkylation or Amination of Allylic Esters (pages 35–57): Maria Zablocka, Marek Koprowski, Jean?Pierre Majoral, Mathieu Achard, Gerard Buono, Jerome Bayardon, Denis Sinou, Matthias Lotz, Gernot Kramer, Katja Tappe, Paul Knochel, Pierluigi Barbaro, Claudio Bianchini, Giuliano Giambastiani and Antonio Togni
Chapter four Suzuki Coupling Reactions (pages 59–90): Ana S. Abreu, Paula M. T. Ferreira, Maria?Joao R. P. Queiroz, Jie Wu, Lisha Wang, Reza Fathi, Zhen Yang, Ramon E. Huertas, John A. Soderquist, Tatsuo Ishiyama, Norio Miyaura, Bin Tao, David W. Boykin, Colin Baillie, Lijin Xu, Jianliang Xiao, Matthew L. Clarke, J. Derek Woollins, Nicholas Marion, Oscar Navarro, Roy A. Kelly and Steven P. Nolan
Chapter five Heck Coupling Reactions (pages 91–112): Peter Nilsson, Mats Larhed, Lijin Xu, Jun Mo, Jianliang Xiao, Tim G. Kilroy, Yvonne M. Malone and Patrick J. Guiry
Chapter 6 Sonogashira Coupling Reactions (pages 113–125): Anupama Datta, Herbert Plenio, Chih?An Lin and Fen?Tair Luo
Chapter 7 Cross?Coupling Reactions (pages 127–153): Jun Terao, Nobuaki Kambe, Luis A. Sarandeses, Jose Perez Sestelo, Bryan A. Frieman, Bruce H. Lipshutz, John Mancuso, Masahiro Yoshida and Mark Lautens
Chapter eight Regioselective or uneven 1,2?Addition to Aldehydes (pages 155–168): Kui?Thong Tan, Shu?Sin Chng, Hin?Soon Cheng, Teck?Peng Loh, Jens Rudolph, Carsten Bolm, Marco Lombardo, Sebastiano Licciulli, Stefano Morganti and Claudio Trombini
Chapter nine Olefin Metathesis Reactions (pages 169–180): Syuzanna Harutyunyan, Anna Michrowska, Karol Grela, Stephen J. Connon, Aideen M. Dunne, Siegfried Blechert, G. Bhaskar and B. Venkateswara Rao
Chapter 10 Cyclisation Reactions (pages 181–200): Jaime Blanco?Urgoiti, Gema Dominguez, Javier Perez?Castells, Ligang Zhao, Xiyan Lu, Minsheng He, Aiwen Lei, Xumu Zhang, Hiroshi Shinokubo, Koichiro Oshima, Antonio Rosales, Juan M. Cuerva and Enrique Oltra
Chapter eleven uneven Aldol and Michael Reactions (pages 201–223): Masakatsu Shibasaki, Shigeki Matsunaga, Naoya Kumagai, Zhuo Tang, Liu?Zhu Gong, Ai?Qiao Mi, Yao?Zhong Jiang, Masahito Watanabe, Kunihiko Murata and Takao Ikariya
Chapter 12 Stereoselective Hydroformylation, Carbonylation and Carboxylation Reactions (pages 225–250): Bernhard Breit, Martin Wills, Simon W. Breeden, Stefania Cserepi?Szucs, Jozsef Bakos, C. Ramesh, Y. Kubota, Y. Sugi, Tomoko Matsuda, Tadao Harada, Toru Nagasawa and Kaoru Nakamura
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Additional info for Catalysts for Fine Chemical Synthesis: Metal Catalysed Carbon-Carbon Bond-Forming Reactions, Volume 3
P. 1, CHCl3). 0 Hz). 7 (CH3). Note: This material is usually of sufficient purity to be used in subsequent reactions, however if required further purification can be achieved by flash chromatography on silica gel (dichloromethane/methanol, 19:1). 5 cm Two Bu¨ chner flasks, 250 mL Two filter papers Rotary evaporator Procedure 1. 09 mmol) in toluene/dichloromethane (40 mL/25 mL). The solution was then placed under a nitrogen atmosphere, and cooled in an ice-water bath. 9M aqueous potassium hydroxide (10 mL) was added dropwise, the ice-water bath removed, and the resulting two-phase mixture was stirred vigorously at room temperature for 16 hours.
Ikonnikov, N. , Maleev, V. I. Tetrahedron 2001, 57, 2491. 2. Belokon’, Y. , Davies, R. , Fuentes, J. , North, M. and Parsons, T. Tetrahedron Lett. 2001, 42, 8093. 3. Belokon’, Y. , Davies, R. G. and North, M. Tetrahedron Lett. 2000, 41, 7245. 4. , Crosby, J. and Peterson, J. A. Tetrahedron Lett. 1999, 40, 8671. 3 ASYMMETRIC PHASE-TRANSFER CATALYSED ALKYLATION OF GLYCINE IMINES USING CINCHONA ALKALOID DERIVED QUATERNARY AMMONIUM SALTS BARRY LYGO* and BENJAMIN I. 2]octane bromide, is a highly effective catalyst in the asymmetric liquid-liquid phase-transfer alkylation of tert-butyl N-(diphenylmethylene)glycinate.
52 ............. 53 ............. ............. 1 SYNTHESIS AND APPLICATION IN PALLADIUMCATALYSED ASYMMETRIC ALLYLIC SUBSTITUTION OF ENANTIOPURE CYCLIC b-IMINOPHOSPHINE LIGANDS MARIA ZABLOCKAa*, MAREK KOPROWSKIa, JEAN-PIERRE MAJORALb*, MATHIEU ACHARDc and GE´ RARD BUONOc* a Centre of Molecular and Macromolecular Studies, Polish Academy of Sciences, Sienkiewicza 112, 90-363 Lodz, Poland b Laboratoire de Chimie de Coordination, CNRS, 205 route de Narbonne, 31077 Toulouse Cedex, France c ENSSPICAM, CNRS, UMR 6516, Faculte´ St Je´ roˆ me, av.